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Separation was performed on a Thermo Scientific Hypersil GOLD aQ reverse phase column (2.1 x 150 mm, 3µm) with a gradient mobile phase system consisting of an aqueous phase of 0.1% formic acid (A) and an organic phase of acetonitrile (B) at a flow rate of 0.5 mL/min (0 - 0.5 min, 0.5-5% B
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